Search results for "Hydroxyl ion"

showing 4 items of 4 documents

Production and Characterization of Oxyhydroxyapatites

2018

The amount and alignment of hydroxyl ions influence the bioactivity of hydroxyapatite. Hydroxyl ions in hydroxyapatite are the most mobile and upon heating are the first to leave the lattice to form oxyhydroxyapatite. This work describes a method for producing hydroxyapatite with different amounts of hydroxyl ions, and reports on the changes in Fourier transform infrared absorption at increasing level of dehydroxylation. Detailed analysis of spectra in the 500 – 700 cm-1 range showed a peak shift for the hydroxyl ion absorption line at 632 cm-1 to 637 cm-1 and an increase in the wavenumber for the phosphate line at 575 cm-1.

Materials scienceMatériaux0206 medical engineeringInorganic chemistryInfrared spectroscopyOxyhydroxyapatite02 engineering and technologyDeconvolution[CHIM.INOR]Chemical Sciences/Inorganic chemistrySpectral lineIonHydroxyapatitechemistry.chemical_compoundsymbols.namesakeGeneral Materials ScienceFourier transform infrared spectroscopyOxyapatiteFourier Transform Infrared SpectroscopyMechanical Engineering[CHIM.MATE]Chemical Sciences/Material chemistry021001 nanoscience & nanotechnologyPhosphate020601 biomedical engineeringHydroxyl IonsFourier transformHydroxyl ion absorptionchemistryMechanics of MaterialssymbolsOxyhydroxyapatite0210 nano-technologyKey Engineering Materials
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Hydrothermal Processing for Increasing the Hydroxyl Ion Concentration in Hydroxyl Depleted Hydroxyapatite

2018

Thermal spraying is commercially used to produce hydroxyapatite coatings, but the high temperature depletes hydroxyl ions in the structure. To return hydroxyapatite to its original state, it is necessary to restore the hydroxyl ion content in the structure. In this work, the effect of hydrothermal treatment on the hydroxyl ions was investigated in hydroxyapatite powder and thermally sprayed hydroxyapatite coatings. Samples were hydrothermally treated at 200 °C for 24 h and 48 h. Chemical phases were determined by X-ray diffraction, functional groups and hydroxyl ion concentration was examined by Fourier transform infra-red spectroscopy. Results showed that hydrothermal processing of hydroxy…

Materials scienceMechanical EngineeringHydrothermal treatment02 engineering and technology010402 general chemistry021001 nanoscience & nanotechnology01 natural sciencesHydrothermal circulation0104 chemical sciencesMechanics of MaterialsGeneral Materials ScienceDeconvolutionFourier transform infrared spectroscopy0210 nano-technologyHydroxyl ionNuclear chemistryKey Engineering Materials
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Crystal structures of bR(D85S) favor a model of bacteriorhodopsin as a hydroxyl-ion pump

2003

AbstractStructural features on the extracellular side of the D85S mutant of bacteriorhodopsin (bR) suggest that wild-type bR could be a hydroxyl-ion pump. A position between the protonated Schiff base and residue 85 serves as an anion-binding site in the mutant protein, and hydroxyl ions should have access to this site during the O-intermediate of the wild-type bR photocycle. The guanidinium group of R82 is proposed (1) to serve as a shuttle that eliminates the Born energy penalty for entry of an anion into this binding pocket, and conversely, (2) to block the exit of a proton or a related proton carrier.

Models MolecularProtein ConformationAnion Transport ProteinsBiophysicsBacteriorhodopsinProtonationCrystal structureCrystallography X-RayBiochemistryIon pumpIonchemistry.chemical_compoundResidue (chemistry)Structural BiologyMutant proteinHydroxidesGeneticsMolecular BiologyIon TransportSchiff basebiologyChemistryBacteriorhodopsinCell BiologyCrystallographyIon pumpBacteriorhodopsinsMutationbiology.proteinHydroxyl ionProtonsFEBS Letters
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Synthesis and Magnetic Properties of a Copper Cube: [Cu 4 (OH) 4 (C 16 H 18 N 2 ) 4 ] 4+ (ClO 4 ) 4 C 3 H 6 O [C 16 H 18 N 2 =( E )‐1,6‐[Di(pyridin‐4…

2019

We are grateful to the National Mass Spectrometry Service Center for mass spectra and to the UK National Crystallography Service for data sets. Supplementary Figure S1-S4: IR and UV/Vis spectra of compound 1

Supplementary dataMaterials science010405 organic chemistrychemistry.chemical_elementGeneral ChemistryVis spectra010402 general chemistryMass spectrometry01 natural sciencesCopper0104 chemical sciencesCrystallographychemistryMass spectrumEne reactionHydroxyl ionChemistryOpen
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